Martin Luther University Halle-Wittenberg

Links

Further settings

Login for editors

Instrumentation

In the section ANM is a wide range of devices. From basic mechanical operations such as crushing and milling using hydraulic press (including powder pellets for sintering experiments) and ball mills, on classical mesh analysis through the sifter (also wet screening up to 5 micron), to the cutting of samples with the help of saws.

Furthermore we can realise supercritical drying of nanoporous samples.

  Abb. 1 Pulverlabor, oben: Analysenwaage, Vakuumpumpe und Siebturm, unten: Fliehkraftkugelmühle, Rollenmischer und Hydraulikpresse

Abb. 1 Pulverlabor, oben: Analysenwaage, Vakuumpumpe und Siebturm, unten: Fliehkraftkugelmühle, Rollenmischer und Hydraulikpresse

 

In the melt and sinter laboratory samples are prepared. There they are thermally treated by high temperature furnaces (until 1750 °C).

  Abb. 2 Schmelz- und Sinterlabor mit Hochtemperaturöfen und einem Klimaschrank

Abb. 2 Schmelz- und Sinterlabor mit Hochtemperaturöfen und einem Klimaschrank

 

The chemical laboratory is used with priority for corrosion tests (statically/dynamically) at glass and building materials.

 

Furthermore become there syntheses (inorganic gels; hydrothermal syntheses) as well as the drying of water-containing materials (e.g. clear fire prevention materials) does. In addition different dry cupboards, special stoves, a climate cupboard (-40 - 180 °C), a coating arrangement (dip – coating), a rotation evaporator and autoclaves (to 450ml) are available to us.

  Abb. 3 Oben links: Hydrothermalsynthese im Drehofen, oben rechts: Autoklaven der Fa. Parr, unten: Trockenschränke und Hochtemperaturofen (vakuumdicht), in der Mitte: Blick durch einen Spezialofen

Abb. 3 Oben links: Hydrothermalsynthese im Drehofen, oben rechts: Autoklaven der Fa. Parr, unten: Trockenschränke und Hochtemperaturofen (vakuumdicht), in der Mitte: Blick durch einen Spezialofen

 

The analytic area of the section ANM is covered as follows: :

    • thermo analysis (DTA/DSC),
    • UV/VIS spectroscopy,
    • dilatometer (e.g. to determine the transformation temperature of glass according to DIN ISO 7884-8:1998-02),
    • volume dilatometer,
    • pyknometer,
    • capillary viscosimeter,
    • falling sphere viscometer,
    • thermal gravimetric analysis,
    • volumetric analyses,
    • ion-selective electrode,
    • pH measuring instruments
    • testing of gypsum according to DIN EN 13279-2:2004-10.

  Abb. 4 v.l.n.r.: ISE, DSC/DTA "STA 409" der Fa. Netzsch, Schubstangendilatometer "DIL 402 C" (1600 °C Version) Fa. Netzsch

Abb. 4 v.l.n.r.: ISE, DSC/DTA "STA 409" der Fa. Netzsch, Schubstangendilatometer "DIL 402 C" (1600 °C Version) Fa. Netzsch

to section

[ more ... ]

Up